CBD Oil Distillation Process

CBDISTILLERY

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How to extract CBD oil – The extraction process & how to make CBD oil CBD (Cannabidiol) is a compound that has shown promise in a variety of medical applications, like relief from pain and In this blog, Maratek gives an overview of the cannabis and hemp oil distillation process and how it can help to create a consistent pure product. Cannabis distillation uses low pressures, gentle heating, and smart evaporation techniques to weed out only the purest cannabinoid liquid oil from crude.

How to extract CBD oil – The extraction process & how to make CBD oil

CBD (Cannabidiol) is a compound that has shown promise in a variety of medical applications, like relief from pain and anxiety which are most common, along with many other ailments. A major benefit to CBD is that it doesn’t contain THC, which is the compound that makes users high, so this makes CBD an ideal product for children. Below you will find a step by step outline of how cbd oil is made.

CBD extract oil from cannabis or hemp.

There are many ways to extract the oil from the plant and make cbd oil. Apeks CO2 extraction systems use CO2 as a solvent to extract the oil. The solvent is considered a cleaner, purer form of extraction because there is no residue after extraction.

To isolate the individual compounds (CBD being one of them), the extracted oil needs to be distilled after extraction. The first step is a process called Winterization, followed by Short Path Distillation.

Winterization

Winterization is the process to remove undesirable elements that were extracted from the plant, for example fats, waxes, and lipids. This process is only needed when the oil was extracted at high pressure/high temperature (supercritical) because this intense extraction pulls everything from the plant, including material you don’t want in the final products. The extracted oil is effectively crude oil, which needs refining.

Once extracted, the mixture is combined with 200 proof alcohol and stirred vigorously until completely mixed. It’s then placed in a deep freezer overnight. In the morning, the mixture looks cloudy and is ready for filtration. One way to filter out the fats, etc. is to run it through a filter paper into an extraction jar. A common piece of equipment for this is a Buchner Funnel. Once it’s been filtered to satisfaction and the undesirable elements have been removed, it’s time to remove the alcohol. This is done using heat. The extraction is warmed and as its warmed, the alcohol evaporates since the boiling point of alcohol is lower than the oil. The removed alcohol may then be used on a different batch of crude oil.

Mixing oil and alcohol prior to freezing

Short Path Distillation equipment

Short Path Distillation

To further refine the CBD extract, and to isolate the CBD, the oil goes through Short Path Distillation. This works in much the same way as Winterization in that the extract is heated and each compound is then separated because each one has a different boiling point. In this way, each compound is isolated and can be used by itself.

Benefits and Uses of CBD

Research is showing that CBD extract has a huge potential in the medical market. CBD’s common benefits are treating anxiety, reducing pain and inflammation, helping prevent seizures, among many others. Because it’s a natural extract, there are few, if any, side effects. The extract works with the body’s endocannabinoid system, which is the system’s method of regulating processes, like pain, mood, appetite, and memory. CBD works with the natural system rather than being an unnatural substance, so the body doesn’t try to reject it. CBD extract may be sourced from cannabis or hemp, most typically from hemp, which is naturally high in CBD. Cannabis can also be bred to have low THC levels and high CBD levels, but it’s possible that the THC will get concentrated and included in your final products.

Tne Entourage Effect

Despite the benefits of CBD as an isolate, there is much to be said for treating patients with all the compounds in the plant, not as separate isolates. Patients can still use the oil without getting high, as long as the THCa has not been heated, which converts it into THC, which is what makes you high. The Entourage Effect is the effect that all the compounds of the plant have on the body, as a whole.

Hemp and cannabis oil extraction processes and techniques.

Andy is on a panel of experts, answering questions from the community. We compiled a collection of questions and answers below, about hemp and cannabis oil extraction processes and techniques.

Click here to get more information on the CBD Extraction Process.

What are the safest and most effective ways to extract and produce CBD-rich cannabis oil? CO2, oil, or ethanol?

Question:
What are the safest and the most effective ways to extract and produce CBD oil? CO2, oil, or ethanol?

Answer:
Thanks for the great question! There are really 2 questions here, so I’ll try to answer them separately.

First question: What are the safest ways to extract? When it comes to extraction, safety is an important issue and has many areas to consider. The list below represents some of the major areas that need to be addressed with the popular solvents being used in the cannabis industry today:

  • Materials of Construction- Stainless steel materials for food/consumed oil applications
  • Electrical for Flammable Solvents – Class 1, Division 1 (explosion proof) electrical components for compressed flammable gasses, Class 1, Division 2 for ethanol/alcohol
  • Electrical, Non Flammable Solvents – NEMA 4x wash down electrical enclosures
  • Pressure Rating – usually 300 psi for hydrocarbons, 2000 or 5000psi for CO2.
  • Overpressure Protection – non-isolable relief valves set to 110% of maximum allowable working pressure
  • Food grade – welds in contact with extracted material should be ground flush and polished
  • Accessibility for Cleaning – vessels and piping should be accessible from both ends to allow proper cleaning
  • Storage tanks – should be stainless steel to prevent corrosion

Facility – In addition to the equipment considerations, the facility must also be appropriate for the extraction solvent.

  • Compressed Flammable Gasses – Class 1, Division 1 facility. This includes electrical fixtures, and also monitoring and evacuation equipment in the event there is a release of flammable gas into the area around the equipment.
  • Ethanol/Alcohol – vent hood or equivalent walk in vent area
  • CO2 – asphyxiation hazard. Monitoring and audible alarm to warn of leaks.
  • CO2 – Generally Regarded as Safe (GRAS) by the FDA for consumption
  • Compressed gas – GRAS for use as a propellant, states differ on safe residual solvent levels
  • Ethanol – GRAS for food products, states differ on safe residual solvent levels
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So the answer to the question about safety really doesn’t have anything to do with the solvent, rather the equipment chosen and the facility where the extraction is performed determine safety. The solvents commonly used in extractions today all have pros and cons, and all can be operated safely as long as proper guidelines and regulations are followed.

I addressed the safety question in the first part of the answer, in the second part I’ll address the efficiency question: What is the most effective way to extract CBD-rich oil?

A major problem facing the cannabis industry today is a lack of commonly accepted standards – as evidenced by the question referring to “CBD-rich”. Does “CBD-rich” mean 40% CBD? 99% CBD? And CBD in what form, CBD, CBD-A or some combination? There are groups that are working towards creating standards, such as FOCUS and ASTM, but they have not been widely accepted yet. Without standards, quality also becomes difficult to determine because the only standard is personal subjectivity.

That being said, there are some generalizations about extraction methods that can be made. Keep in mind – every extraction method has benefits and drawbacks. Each method will shine in certain applications, and perform poorly in other. No method is great at everything.

An Overview of the Cannabis and Hemp Oil Distillation Process

Are you looking to improve your cannabis and hemp oil extraction methods? In this blog, Maratek is going to give an overview of the cannabis and hemp oil distillation process and how it can help to create a consistent pure product.

What is distillation?

Distillation is a process that heats a substance into a vapor and cools it back to a liquid. This process can be used to separate components with different boiling points. There are different variations of this process, which are all dependent on the components, and the temperature, and pressure of the system.

Simple distillation is appropriate for the separation of materials that have significantly different boiling points. When heated the liquid that is more volatile will vaporize and travel through the system, recondensing into a liquid when it passes through a chilled condenser. This results in the volatile substance becoming separated from the initial product.

How is distillation used for cannabis oil?

The cannabis and hemp industry uses distillation to further purify crude oil. The extraction process generally uses solvents such as ethanol, or CO2 to remove the crude oil from the plant biomass. The distillation equipment then takes the crude oil and produces a pure product, usually of either THC or CBD distillate by removing other volatiles and contaminants.

Distillation can take multiple passes to remove all unwanted compounds before producing the intended final product. The first pass usually removes low boiling point volatiles. A second pass focuses on distilling the desired cannabinoids, leaving behind other contaminants such as waxes, sugars and any leftover plant material. This results in a pure product of the desired cannabinoids or terpenes depending on a company’s intention.

Multiple passes can be necessary especially if a company does not use a winterization process on their products . Winterization removes any contaminants like fats, and waxes from the initial oil extraction. Without this process those contaminants are left in the solution and will need to be removed during distillation to produce a pure final product. Setting up multiple distillation equipment that are connected directly to each other reduces the need for multiple passes through a singular system.

The most common form of distillation system is short path distillation. It is beneficial because the vapor travels a shorter distance before it is condensed, allowing the equipment to take up less space. The crude oil is deposited at the bottom of a flask where it is then heated to initiate the distillation process. This system generally gets used on a smaller scale, as it typically needs more manual operation or oversight.

A similar equipment is the wiped film distillation system. The only difference to the above system is the introduction of a wiper blade that spreads a layer of the initial feed product onto the chamber walls. This thin layer reduces the amount of time heat is applied to the product. Prolonged exposure to heat can degrade a cannabis product and this equipment reduces that risk. The wipers also provide an even spread that supports more consistent evaporation and condensation rates.

The popularity of wiped film short path distillation may also be attributed to its continuous feed abilities that increase output and efficiency. Continuous feed supports operation by helping to produce large quantities and maintaining consistency. This process is more automated due to continuous feed and the wipers and is therefore more suitable for large scale operations.

Temperatures and pressures used in a system can usually be altered to address a business’s specific goals. Changing the pressure can affect the temperatures at which certain compounds boil at, making it easier to remove them from the product. If boiling temperatures are lowered, this also decreases the risk of overheating and degrading the product.

Distillation is relatively simple once the extraction process has taken place. After all the undesirable materials are removed during the extraction process, the purest form of crude oil is left. As this is not a one size fits all method, the industry today requires you to focus on both scaling up for the mass market, and scaling down for smaller, more local needs.

As short path distillation requires less pressure to be exerted on the distillate, it is more common and favorable when working with volatile compounds and when purifying small amounts of substance. With heat, pressure, and humidity – it forces the remaining impurities and traces of solvent extraction residue out.

The short path causes the cannabis extract to break down into its constituent compounds. THC and CBD are separated out at different temperatures as they have slight differences in boiling points. It is more effective and has better results when it is done on a large scale using industrial level equipment. Once it is distilled, the cannabis concentrate has a higher CBD or THC content compared to the crude oil. Distillates of different cannabinoids can then be blended to customize a product.

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If further purification is required, the distillate can be passed through an isolate production system to obtain up to 99.9% pure cannabinoids.

Want to learn more about the process of distillation in the cannabis and hemp extraction industry? Maratek has engineered short path distillation systems that will improve the purity of your product. Contact us today for more information .

Cannabis Distillate: Behind the Making of Pure & Potent Liquid Gold

Cannabis distillates are the ultra-refined extracts from the cannabis plant found in vape cartridges, edibles, and topical products worldwide. Distillates contain a single cannabinoid in pure and potent oil. Their amber-colored and translucent appearance does not start off that way. A series of extraction and purification processes convert the raw cannabis and hemp plant material into the marijuana distillate found in a significant amount of cannabinoid-based products.

In a world full of flavorful and aromatic full-spectrum concentrates, why does cannabis distillate seem to be everywhere? Why is this scentless and flavorless extract so coveted among producers? Our cannabis distillate guide breaks down the different distillate types, how they are made, and how they are used for medical and recreational use around the world.

What Is Cannabis Distillate?

As a new user, it can get confusing trying to wrap your head around the different types of cannabis extracts available. Simply put, cannabis distillate is a type of cannabis extract that has gone through a distillation process to create a pure product with nearly 100% CBD or THC content. During the distillation process, processors use distillation equipment to separate the targeted compound, particularly THC or CBD, from the solvent, and other compounds.

Cannabis and hemp are composed of hundreds of individual compounds including cannabinoids, terpenes, flavonoids, and other essential oils. In the end product, boiling techniques remove nearly all of the flavor and aroma that comes from the plant’s terpenes. While terpenes are believed to elevate cannabinoids’ therapeutic potential, they are not always welcome.

Since all of the wax, lipid, and undesirable plant matter is removed from the extract, distillates take on a translucent look. Its viscous and sticky consistency contains a nearly pure potency reaching up to 98% cannabinoids compared to the slightly lower levels (60 to 80%) of undistilled extracts.

THC Distillate

For high tolerance users or medical marijuana patients needing high doses of the inflammation- and pain-fighting tetrahydrocannabinol (THC) compound, THC distillate boasts an impressively high concentration of the intoxicating THC. Its psychotropic and euphoric effects can help treat pain, muscle spasticity, glaucoma, insomnia, low appetite, nausea, and anxiety.

CBD Distillate

Cannabidiol (CBD) offers a more subdued and non-intoxicating alternative to the cerebral effects of THC. CBD distillate contains no THC and a nearly pure concentration of CBD. CBD distillate is a powerful extract meant to reap all of cannabis’ and hemp’s wellness benefits without the high. CBD has been shown to help treat seizures, inflammation, pain, nausea, depression, anxiety, and migraines.

Terpenes and Flavonoids

Cannabis terpenes are responsible for the unique aroma of each cannabis plant strain. While terpenes are found in minor levels in the cannabis plant compared to cannabinoids, they offer a robust aroma that can fill a room. Flavonoids are found in even lesser amounts and are responsible for the colors in your buds. Removing these compounds helps processors produce a uniform extract that can be flavored afterward.

What Is the Difference Between Distillate, Oil, and Isolate?

Cannabis oil goes by so many names, it is hard to keep track. Cannabis distillate always takes on a viscous oil consistency. It is a type of cannabis oil, but not all cannabis oils are distillates. The term distillate is reserved for oils that have undergone a distillation process after the oil has been extracted, winterized, and decarboxylated. Cannabis oils such as live resin, butane hash oil (BHO), Rick Simpson Oil (RSO), or hemp-derived CBD oil are similar but not the same.

Many people confuse distillate and isolate since they both focus on a single cannabinoid. In fact, isolate is technically a type of distillate since distillation techniques are used to refine the cannabinoid extract. Cannabinoid isolates, however, are completely pure crystalline powder forms of the therapeutic compound. Think of distillate as a less refined but equally powerful extract that elicits potent effects.

How Is Distillate Made?

Making cannabis distillate starts with a cannabis or hemp seed and undergoes a range of cultivation, extraction, and post-processing steps to remove the cannabinoids, terpenes, and flavonoids from the biomass (flowers, leaves, and stems). Here is a complete rundown of the supply chain and process used to distill the most valuable cannabis compounds.

Extraction Process

Even before the distillation process is initiated, the cannabis plant must undergo multiple steps including being properly dried and cured after harvest. Once dried, the biomass can be extracted using a range of solvents including carbon dioxide, butane, and ethanol. The biomass is packed in a material column, drenched in the solvent, and may be further refined using color remediation techniques before ending up in the collection tank.

Some processors may perform a winterization on their extracts to remove fats and waxes using ethanol and cold temperatures. In addition, the extract may be decarboxylated to activate the acidic cannabinoids, such as THCA and CBDA, into their parent compounds: CBD and THC.

In the end, crude oil derived from the initial cannabis extraction process contains a THC or CBD concentration between 60 and 80%. The rest of the oil will be composed of different flavors and aromas (terpenes), vitamins, antioxidants, and other essential oils. After the extraction process, the oil needs to be further purified to become a distillate.

Distillation Process

Cannabis distillation equipment varies but the process is very similar among the different distillation methods. Distillation reduces the pressure inside the apparatus to purify the cannabinoid at the lowest possible boiling point. A distillation apparatus heats the cannabis oil to a specific temperature to evaporate the desired cannabinoid from the oil without degrading it and then condensing the cannabinoid vapor back into a liquid.

Through steam distillation and fractionation techniques, distillation equipment can remove the ethanol, carbon dioxide, or butane solvent and almost everything else besides the cannabinoid through multiple passes.

Generally, the short exposure to heat during the process reduces the risk of degrading the highly volatile cannabis compounds. In addition, the best equipment creates a thin film of the oil onto the evaporative surface for more uniform heating and evaporation. Compounds with higher boiling points usually fall downward with the force of gravity and agitation into a separate residual collection vessel.

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Distillation Equipment

Cannabis distillation equipment ranges from small units for small-batch operators to industrial-scale models for larger operations. Running the crude extract through the equipment multiple times helps remove as much of the plant matter, terpenes, and flavonoids as possible. The first “pass” removes volatile solvents, gases, and water while additional passes remove terpenes and flavonoids from the final product.

Short Path Distillation

Short path distillation, also known as fractional distillation, is a purification method that uses vacuum pressure to lower the boiling points of the cannabinoids and terpenes. Since lower temperatures are used, the gentle short path distillation can carefully weed out the cannabinoids and terpenes from the end product without damaging them.

Short path distillation uses slow thermal heating to heat crude oil in a glass flask with a magnetic stirrer. As the temperature slowly rises, extractors can separate fractions of the distillate beginning with the terpenes and solvent. Each fraction is collected in a collection flask. There are usually three, one for terpenes and highly volatile compounds, another for CBD or THC, and the last one for cannabinoids with high boiling points.

Wiped Film Distillation

Wiped film distillation is a type of short path distillation. Under a vacuum, the cannabis oil is loaded onto a heated and rotating vertical cylinder. Wipers continuously wipe the extract creating a thin film on the evaporative surface. A chilled condenser in the center of the wipers condenses the THC or CBD vapor. Different collection vessels collect the CBD or THC distillate and any heavier compounds such as chlorophyll, wax, and salts below.

Rotary Evaporation

Rotary evaporation techniques use rotary evaporators, also known as roto-vaps, are common in the removal of the solvent from the final product. In a rotary evaporator, the pressure drops using a vacuum pump which reduces the boiling point of the solvent. A rotating distilling flask is filled halfway and heated using a water bath. The distillation flask is rotated creating a thin film of the cannabis concentrate. This increases its surface area to speed up the evaporation rate.

Falling Film Evaporation

Falling film evaporators include an evaporator and condenser and use a different boiling point to separate compounds from the cannabis concentrates. Using this method, the oil is drained from above into a heated column and falls downward creating a thin film on the evaporative surface. As the cannabinoids evaporate, they are collected on a chilled condenser. Due to its unique methodology, cannabinoid products with lower viscosity work well under this process.

How to Use Cannabis Distillates

THC and CBD distillate can be used in a variety of ways for medicinal and recreational consumption. Its versatility makes it a favorite among extraction companies and consumers. Smoke it, vape it, cook with it, or make soothing lotions and creams infused with THC or CBD. The possibilities are endless. Cannabis distillate can be found in a majority of products sold in retail shops today.

Dab Rig/Portable Vaporizer

Cannabis concentrates such as distillates are commonly consumed, or dabbed, with a glass dab rig or electronic nail (e-nail). Dab rigs and e-nails are great for use at home since they can deliver large doses using heated surfaces. E-nails, in particular, can maintain consistent temperatures using a digital controller and power source to perfectly vaporize cannabis oil. E-nails offer the convenience of not having to use a torch and estimate your heat up and cool down times for your nail.

Portable vaporizers and certain battery-operated vape pens are good for on-the-go consumption. Many vape pen cartridges contain CBD or THC distillate (some with additional flavors) that can be disposed of when finished. Other portable vape pens feature a heating chamber that can be reloaded with a CBD or THC distillate.

Pipes, Bongs, Joints

While dabbing distillates is the recommended method of consumption for sky-high potencies, many users may also smoke their distillates to enhance the potency of their dried cannabis flower. Simply add a tiny dollop of your cannabis oil on top of a packed bowl or within/outside your joint for an enhanced effect.

Edibles

Cannabis distillates are a favorite ingredient in the making of edible products. Distillates can be infused into your favorite foods or beverages. Add this already decarboxylated oil directly onto your finished meal or use it as an ingredient as you cook. A distillate’s flavorless and odorless form allows you to create edible products that do not have the tell-tale taste and smell of the cannabis plant.

In addition, you can consume distillate sublingually for faster absorption and onset of effects compared to ingestion. It is recommended to bind the distillate to a carrier fat such as coconut oil, MCT oil, butter or other food-grade oil for better absorption since THC cannabinoids bind to fat. While the extract is already decarboxylated, it still needs help absorbing into the mucous membranes under the tongue. Warm up the mixture, stir until it is dissolved, and it is ready to go.

Topicals

No matter what cannabinoid distillate you buy or produce, you can infuse it into a variety of topical products including lotions, creams, and salves. Recipes require cannabis distillates and a carrier oil such as coconut oil along with your favorite essential oils for aroma. The salve infused with cannabinoids can be applied directly to the affected area for localized relief without the high since the cannabinoids cannot reach the blood-brain barrier.

Why is Distillation Important?

Through distillation, operators can purchase a greater volume of marijuana trim or low-quality biomass and distill their desired compounds into an ultra-potent liquid.

Distillates have become the backbone of the marijuana derivatives market. Find them in nearly every product category. Their flavorless and scentless characteristics help create a consistent and repeatable cannabinoid product.

Those infused gummies and chocolates we all know and love are only possible with a foundation of distillates. And, if you are a fan of aromatic terpene compounds, they can be reintroduced back into the final product.

Luna Technologies: Automated Cannabis Extraction

High-quality THC and CBD distillate require an efficient extraction stage to remove as much of the cannabinoids from the cannabis plant. Luna Technologies’ automated extraction system, the IO Extractor, provides processors with a peer-reviewed hydrocarbon solution. Produce clean and pure marijuana distillates from any quality cannabis or hemp biomass using the power of hydrocarbons and automation.

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